2022-Spring Synthesis Laboratory (CHEM325-01) The course syllabus

1.Course Information

Course No. CHEM325 Section 01 Credit 2.00
Category Major required Course Type Classroom Course prerequisites CHEM226 (Chemical Reaction Laboratory)
Postechian Core Competence
Hours MON / 14:00 ~ 17:50 / Laboratory Building I[206] Grading Scale G

2. Instructor Information

Ahn Yangsoo Name Ahn Yangsoo Department Dept. of Chemistry
Email address ysahn@postech.ac.kr Homepage
Office Office Phone 054-279-8620
Office Hours 매일 10:00~12:00, 화,목,금 14:00~17:00

3. Course Objectives

The purpose of this course is to provide a chance to experience organic and inorganic synthesis, and to acquaint the students with experimental procedures and techniques.

4. Prerequisites & require

화학과 2017학번 이전의 학생들은 수강이 불가능함.

필수 선수과목: Chemical Reaction Laboratory (화학반응실험)
*유기화학실험(CHEB211) 이수자도 수강 가능 (단, 유기화학실험의 화학과 전공 인정 여부와 별개 사항임)
추천 선수과목 1) Organic Chemistry I & II
2) Inorganic Chemistry

* 당해 학기 실험실 안전교육을 이수해야 실험 수업에 참여할 수 있음.

5. Grading

1) Report : - Pre-Report : 100 pt, - Inlab report : 250 pt, - Final Report : 100 pt
2) Inlab activities : 150 pt (Comprehension/Concentration, Rapidity, Attitude, Cleanliness, Safety etc)
3) Quiz : 120 pt
4) Examination : 180 pt
5) Experimental Report : 100 pt (2 reports)

6. Course Materials

Title Author Publisher Publication
Year/Edition
ISBN
Synthesis Laboratory 안양수 POSTECH 0000 978-89-92231-36-7

7. Course References

1. D. L. Pavia, G. M. Lampman, G. S. Kriz and R. G. Engel, Introduction to Organic Laboratory Techniques-A Small Scale Approach, 2nd ed., Brooks/Cole, Belmont, CA, 2005.
2. R. J. Angelici, :Synthesis and Technique in Inorganic Chemistry", 2nd Ed., W.B.Sanders, 1986.
3. Your Textbooks

8. Course Plan

* 아래의 11개 실험 중 유기, 무기 부분 각각 3개씩 6개의 실험을 진행함.
* CHEM321과 같이 진행하므로 실험 순서는 변경될 수 있음.
* 다른 실험으로 대체될 수 있음 (해당 실험 실시 3~4주전에 공지)

1 : Orientation & Check-in
2 : Natural Product Isolation
3 : Diazo coupling reaction
4 : Enamine Condensation
5 : Preparation of Mn(salen) complex
6 : Asymmetric Synthesis (1)
7 : Asymmetric Synthesis (2)
8 : Asymmetric Synthesis (3)
9 : Synthesis & Magnetic Properties of [Cr(NH3)6](NO3)3
10 : Catalytic Isomerization
11 : Preparation & Optical Resolution of Co(en)3+ complex
12 : Preparation of Macrocyclic Compound
13 : Check-out
14 : Final Examination

9. Course Operation

1) 수업은 매주 월요일 오후 2시 부터 제1실험동 합성실험실에서 진행함.
2) 필요한 경우에는 수요일 오후 시간에 수업할 경우도 있음.
3) 각 실험은 은 퀴즈, 발표 및 실습의 순으로 진행함.
4) 실험실 안전 및 수업 운영에 관한 동의서를 작성하여 제출해야 함

10. How to Teach & Remark

1) 수업에 임하기 전에 교재의 내용에 따라 실험 준비를 충실히 할 것.
2) 규정된 실험 복장을 갖출 것.

11. Supports for Students with a Disability

- Taking Course: interpreting services (for hearing impairment), Mobility and preferential seating assistances (for developmental disability), Note taking(for all kinds of disabilities) and etc.

- Taking Exam: Extended exam period (for all kinds of disabilities, if needed), Magnified exam papers (for sight disability), and etc.

- Please contact Center for Students with Disabilities (279-2434) for additional assistance